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The Journal of Organic Chemistry

Acid-catalyzed addition of secondary amines to cyclopropyl ketones. Mass spectra of some cyclic aminobutyrophenones

J Yovell, D Hirsch, S Sarel

文献索引:Yovell,J. et al. Journal of Organic Chemistry, 1977 , vol. 42, p. 850 - 855

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被引用次数: 7

摘要

850 J. Org. Chem., Vol. 42, No. 5, 1977 Yovell, Hirsch, and Sarel authentic sample. The aqueous layer was acidified (hydrochloric acid) and extracted (ether). Evaporation of ether gave 0.41 g (68%) of diphenylacetic acid (13). Recrystallization of 13 from benzene gave colorless granules, mp 147-148" C. The melting point and IR spectrum of 13 were in good agreement with those of an authentic sample.