The Journal of Organic Chemistry

. alpha.-Methoxylation of Unsaturated Carbonyl Compounds

A Feuerer, T Severin

文献索引：Feuerer, Albert; Severin, Theodor Journal of Organic Chemistry, 1994 , vol. 59, # 20 p. 6026 - 6029

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被引用次数: 8

摘要

General Procedure for the Synthesis of (Ethoxycarbony1) hydrazones 8. The appropriate carbonyl compound (20.0 mmol) was added to a solution of ethoxycarbonylhydrazine (20.0 mmol) and glacial acetic acid (10 drops) in EtOH (20 mL). The mixture was stirred at rt for 24 h. The volatile materials were removed in vacuo and the crude product recrystallized from a suitable solvent.