The Journal of organic chemistry

Al-isopropoxydiisobutylalane: A study of the effect of solvent on the rate and stereoselectivity of cyclic ketone reduction

PS Bahia, MA Jones, JS Snaith

文献索引：Hueckel,W.; Moegle,E. Justus Liebigs Annalen der Chemie, 1961 , vol. 649, p. 13 - 20

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被引用次数: 15

摘要

... e Reaction performed at −78 °C; ratio at 25 °C was 71:29. f Ratio measured by HPLC. ... Thus, a solution of DIBA i OPr in toluene was prepared as before, and diluted with 20 times its volume of ether before addition of 3,3,5-trimethylcyclohexanone. ...