The Journal of organic chemistry

Development of a bio-inspired acyl-anion equivalent macrocyclization and synthesis of a trans-resorcylide precursor

SM Mennen, SJ Miller

文献索引：Elphimoff-Felkin,I.; Verrier,M. Bulletin de la Societe Chimique de France, 1967 , p. 1047 - 1052

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被引用次数: 29

摘要

... entry 4). With potassium tert-butoxide, triazolium salt 11 provided 16% yield (entry 5), whereas lithium hexamethyldisilazide at 56 °C in toluene afforded a 9% yield of 6 (entry 6). Diluting a 2.5:1 mixture of methylene chloride/tert-butanol from 0.01 to 0.0025 M and utilizing DBU ...