Journal of the American Chemical Society

Peroxydisulfuryl Difluoride

FB Dudley, GH Cady

文献索引：Dudley, F. B.; Cady, G. H. Journal of the American Chemical Society, 1957 , vol. 79, p. 513 - 514

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被引用次数: 66

摘要

During the preparation of some fluorine fluorosulfonate,* bp-31.3'by the action of fluorine on sulfur trioxide, a small amount of a reactive byproduct, liquid at room temperature, was obtained. The object of this investigation was to vary the reaction conditions in an effort to obtain this new compound in sufficient quantity to permit identification. A decrease in temperature was found to decrease the yield of fluorine fluorosulfonate but to increase the ...