... Chem. ... The organic layer was washed further with aqueous citric acid (2 X 100 mL), 1 N NaHC03 (2 X 100 mL), and saturated aqueous NaCl(100 mL). ... when the mixture was allowed to stand: mp 74-76 OC: NMR (CDC1,) 6 1.43 (s,9), 1.2-2.1 (m, 8), 2.07 (s, 3), 2.54 (t, 2, J = 7 Hz ...