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Synlett

Preparation of sulfenyl pyrroles

HM Gillis, L Greene, A Thompson

文献索引:Gillis, H. Martin; Greene, Lana; Thompson, Alison Synlett, 2009 , # 1 p. 112 - 116

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被引用次数: 12

摘要

Abstract Sulfenyl groups are attracting interest as masking/protecting groups for pyrroles. A facile one-step synthesis of sulfenyl pyrroles, involving the reaction of pyrroles with N-(aryl- and alkylthio) phthalimides in the presence of MgBr 2, is reported and the methodology extends to include sulfinyl pyrroles. The one-step procedure gives good yields and is more efficient and practical than current multistep protocols to sulfenyl pyrroles that involve ...