Chemistry of the sulfur-nitrogen bond. VIII. N-Alkylidenesulfinamides

FA Davis, AJ Friedman, EW Kluger

文献索引：Davis,F.A. et al. Journal of the American Chemical Society, 1974 , vol. 96, p. 5000 - 5001

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被引用次数: 57

摘要

Silver hyponitrite is the starting material for the synthesis of alkyl hyponitrites, which are useful low-temperature sources of alkoxy radicals. l-5 Numerous syntheses of sodium and silver hyponitrites have appeared in the literat~ re-j-~ Most are tedious, hazardous, poorly described, or require large quantities of mercury. In our hands, one procedure gave no product and the reaction mixture from another ignited during work-up. The method ...