Tetrahedron

A convenient and practical method for the selective benzoylation of primary hydroxyl groups using microwave heating

S Caddick, AJ McCarroll, DA Sandham

文献索引：Caddick, Stephen; McCarroll, Andrew J; Sandham, David A Tetrahedron, 2001 , vol. 57, # 29 p. 6305 - 6310

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被引用次数: 29

摘要

... Tetrahedron. Volume 57, Issue 29, 16 July 2001, Pages 6305–6310. ... Received 20 February 2001, Revised 3 May 2001, Accepted 24 May 2001, Available online 19 July 2001. ... mp 39–40°C. ν max (Nujol) 3507 (O–H), 1697 cm −1 (CO). δ H 0.88 (3H, m, CH 3 ), 1.0–1.5 (12H, m), 2.15 (1H, s, OH), 3.86–4.04 (1H, m, CH), 4.23 (1H, dd, J 1 =7.2 Hz, J 2 =11.5 Hz, OHCH), 4.40 (1H, dd, J 1 =7.2 Hz, J 2 =11.5 Hz, OHCH), 7.40–7.60 (3H, m, ArH), 8.02–8.10 (2H, m, ArH). ...