Journal of Heterocyclic Chemistry

Facile synthesis of 2, 5??diacylthiophenes

Y Miyahara

文献索引：Miyahara,Y. Journal of Heterocyclic Chemistry, 1979 , vol. 16, p. 1147 - 1151

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被引用次数: 47

摘要

Abstract A base-catalyzed condensation of diketo sulfides [(RCOCH 2) 2 S] with glyoxal affording 2, 5-diacylthiophenes has been effected under mild conditions. Excellent results were readily obtained when R was various substituted phenyl, thienyl, or t-butyl groups. Although the yield for R= methyl was poor, the increase in length of the aliphatic chain markedly increased the yields.