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丁基邻苯二甲酰羟乙酸丁酯

丁基邻苯二甲酰羟乙酸丁酯用途

自组装材料，接触印刷材料

丁基邻苯二甲酰羟乙酸丁酯名称

[ CAS 号 ]:
85-70-1

[ 中文名 ]:
丁基邻苯二甲酰羟乙酸丁酯

[ 英文名 ]:
2-Butoxy-2-oxoethyl butyl phthalate

[中文别名 ]:

[英文别名 ]:

MFCD00053793
2-Butoxy-2-oxoethyl butyl phthalate
Butylphthalyl butylglycolate (BPBG)
EINECS 201-624-8

丁基邻苯二甲酰羟乙酸丁酯物理化学性质

[ 密度 ]:
1.1±0.1 g/cm3

[ 沸点 ]:
428.4±25.0 °C at 760 mmHg

[ 分子式 ]:
C₁₈H₂₄O₆

[ 分子量 ]:
336.380

[ 闪点 ]:
185.5±23.2 °C

[ 精确质量 ]:
336.157288

[ PSA ]:
78.90000

[ LogP ]:
4.46

[ 外观性状 ]:
液体;Colorless to Light yellow to Light orange clear liquid

[ 蒸汽压 ]:
0.0±1.0 mmHg at 25°C

[ 折射率 ]:
1.501

[ 储存条件 ]:
仓库通风低温干燥

[ 水溶解性 ]:
水溶性：不溶

丁基邻苯二甲酰羟乙酸丁酯MSDS

详细MSDS(安全技术说明书)

丁基邻苯二甲酰羟乙酸丁酯毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: TI0535000

CHEMICAL NAME :: Phthalic acid, butyl ester, ester with butyl glycolate

CAS REGISTRY NUMBER :: 85-70-1

BEILSTEIN REFERENCE NO. :: 2007363

LAST UPDATED :: 199710

DATA ITEMS CITED :: 16

MOLECULAR FORMULA :: C18-H24-O6

MOLECULAR WEIGHT :: 336.42

WISWESSER LINE NOTATION :: 4OV1OVR BVO4

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: Standard Draize test

ROUTE OF EXPOSURE :: Administration into the eye

SPECIES OBSERVED :: Rodent - rabbit

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Oral

SPECIES OBSERVED :: Rodent - rat

DOSE/DURATION :: 7 gm/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Intraperitoneal

SPECIES OBSERVED :: Rodent - rat

DOSE/DURATION :: 6889 uL/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Oral

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 12567 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Intraperitoneal

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 6880 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :: TDLo - Lowest published toxic dose

ROUTE OF EXPOSURE :: Intraperitoneal

DOSE :: 2296 mg/kg

SEX/DURATION :: female 5-15 day(s) after conception

TOXIC EFFECTS :: Reproductive - Fertility - post-implantation mortality (e.g. dead and/or resorbed implants per total number of implants)

TYPE OF TEST :: TDLo - Lowest published toxic dose

ROUTE OF EXPOSURE :: Intraperitoneal

DOSE :: 689 mg/kg

SEX/DURATION :: female 5-15 day(s) after conception

TOXIC EFFECTS :: Reproductive - Effects on Embryo or Fetus - fetotoxicity (except death, e.g., stunted fetus) Reproductive - Specific Developmental Abnormalities - musculoskeletal system

MUTATION DATA

TYPE OF TEST :: Cytogenetic analysis

TEST SYSTEM :: Rodent - hamster Fibroblast

DOSE/DURATION :: 125 mg/L/24H

REFERENCE :: MUREAV Mutation Research. (Elsevier Science Pub. B.V., POB 211, 1000 AE Amsterdam, Netherlands) V.1- 1964- Volume(issue)/page/year: 48,337,1977 *** REVIEWS *** TOXICOLOGY REVIEW RREVAH Residue Reviews. (Springer-Verlag New York, Inc., Service Center, 44 Hartz Way, Secaucus, NJ 07094) V.1- 1962- Volume(issue)/page/year: 54,1,1975 *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOHS - National Occupational Hazard Survey (1974) NOHS Hazard Code - M1131 No. of Facilities: 156 (estimated) No. of Industries: 5 No. of Occupations: 6 No. of Employees: 2714 (estimated) NOES - National Occupational Exposure Survey (1983) NOES Hazard Code - M1131 No. of Facilities: 10 (estimated) No. of Industries: 2 No. of Occupations: 2 No. of Employees: 431 (estimated) No. of Female Employees: 49 (estimated)

丁基邻苯二甲酰羟乙酸丁酯安全信息

[ 危害码 (欧洲) ]:
N-T

[ 风险声明 (欧洲) ]:
62-61-51

[ 安全声明 (欧洲) ]:
S61-S53-S45

[ RTECS号 ]:
TI0535000

[ 海关编码 ]:
2917349000

丁基邻苯二甲酰羟乙酸丁酯合成路线

详细合成路线

丁基邻苯二甲酰羟乙酸丁酯上下游产品

丁基邻苯二甲酰羟乙酸丁酯上游产品

丁基邻苯二甲酰羟乙酸丁酯下游产品

丁基邻苯二甲酰羟乙酸丁酯制备

（1）将苯酐和丁醇按摩尔比为1：1.05的比例投入反应釜，搅拌下升温至100℃左右进行单酯化，生成邻苯二甲酸单丁酯。

（2）将氯乙酸和丁醇按摩尔比为1：1.2的比例投入反应釜，搅拌下升温至（140±5）℃进行反应，生成氯乙酸丁酯。

（3）将上述制备的邻苯二甲酸单丁酯、氯乙酸丁酯和碳酸钠按摩尔比为1：1.1：0.6的比例投入反应釜，搅拌下升温至150℃进行缩合。粗品用60-70℃的水进行水洗，再用10%的纯碱液进行碱洗，再用水洗后，加入薄膜蒸发。再用质量约为丁酯质量的2%的活性炭于80-90℃下脱色，最后经压滤即得成品。

丁基邻苯二甲酰羟乙酸丁酯海关

[ 海关编码 ]: 2917349000

[ 中文概述 ]:
2917349000 其他邻苯二甲酸酯。监管条件:无。增值税率:17.0%。退税率:9.0%。最惠国关税:6.5%。普通关税:30.0%

[ 申报要素 ]: 品名, 成分含量, 用途, 对苯二甲酸请注明4-CBA值, 对苯二甲酸请注明P-TL酸值, 对苯二甲酸请注明色度, 对苯二甲酸请注明水分

[ Summary ]:
2917349000 other esters of orthophthalic acid。Supervision conditions:None。VAT:17.0%。Tax rebate rate:9.0%。MFN tariff:6.5%。General tariff:30.0%