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氯(代)正己烷

氯(代)正己烷用途

【用途一】
用于有机合成
【用途二】
用于香料的合成

氯(代)正己烷名称

[ CAS 号 ]:
544-10-5

[ 中文名 ]:
1-氯己烷

[ 英文名 ]:
chlorohexane

[中文别名 ]:

[英文别名 ]:

N-Chlorohexane
1-Chlorhexan
MFCD00001018
n-Hexylchlorid
1-hexyl chloride
Hexane, chloro-
Hexylchlorid
HEXYL CHLORIDE
Hexane, 1-chloro-
1-chloro-hexan

氯(代)正己烷物理化学性质

[ 密度 ]:
0.9±0.1 g/cm3

[ 沸点 ]:
133.9±3.0 °C at 760 mmHg

[ 熔点 ]:
−94 °C(lit.)

[ 分子式 ]:
C₆H₁₃Cl

[ 分子量 ]:
120.620

[ 闪点 ]:
26.7±0.0 °C

[ 精确质量 ]:
120.070580

[ LogP ]:
3.63

[ 外观性状 ]:
无色液体,芳香气味

[ 蒸汽压 ]:
10.2±0.2 mmHg at 25°C

[ 折射率 ]:
1.414

[ 储存条件 ]:
Flammables area

[ 稳定性 ]:
Stable. Flammable. Incompatible with strong oxidizing agents, strong bases.

氯(代)正己烷MSDS

氯(代)正己烷安全信息

[ 符号 ]:

GHS02

[ 信号词 ]:
Warning

[ 危害声明 ]:
H226

[ 个人防护装备 ]:
Eyeshields;Faceshields;full-face respirator (US);Gloves;multi-purpose combination respirator cartridge (US);type ABEK (EN14387) respirator filter

[ 危害码 (欧洲) ]:
Xi:Irritant;

[ 风险声明 (欧洲) ]:
R10;R20/21;R37

[ 安全声明 (欧洲) ]:
S23-S24/25-S16-S61-S60

[ 危险品运输编码 ]:
UN 1993 3/PG 3

[ WGK德国 ]:
1

[ 包装等级 ]:
III

[ 危险类别 ]:
3

[ 海关编码 ]:
29031980

氯(代)正己烷合成路线

氯(代)正己烷上下游产品

氯(代)正己烷上游产品

氯(代)正己烷下游产品

氯(代)正己烷制备

1.制法：

于装有搅拌器、回流冷凝器、滴液漏斗的反应瓶中，加入氯化亚砜110mL(1.5mol),慢慢滴加51g(0.5mol)己醇-1(2),约2h加完。滴加过程中有二氧化硫和氯化氢气体逸出，注意用稀碱吸收，并反应液颜色变深。加完后回流反应2h。改为蒸馏装置，蒸出氯化亚砜。再收集132～134℃的馏分。镏出液依次用水、10%的碳酸钠、水洗涤，无水氯化钙干燥，分馏，收集133～134℃的馏分，得1-氯己烷(1)35g，收率60%。

氯(代)正己烷海关

[ 海关编码 ]: 2903199000

[ 中文概述 ]:
2903199000 其他无环烃的饱和氯化衍生物。监管条件:无。增值税率:17.0%。退税率:9.0%。最惠国关税:5.5%。普通关税:30.0%

[ 申报要素 ]: 品名, 成分含量, 用途

[ Summary ]:
2903199000 other saturated chlorinated derivatives of acyclic hydrocarbons。Supervision conditions:None。VAT:17.0%。Tax rebate rate:9.0%。MFN tariff:5.5%。General tariff:30.0%

氯(代)正己烷文献

QSPR modeling of octanol/water partition coefficient for vitamins by optimal descriptors calculated with SMILES.

Eur. J. Med. Chem. 43 , 714-40, (2008)

Simplified molecular input line entry system (SMILES) has been utilized in constructing quantitative structure-property relationships (QSPR) for octanol/water partition coefficient of vitamins and org...

Evaluation of injection methods for fast, high peak capacity separations with low thermal mass gas chromatography.

J. Chromatogr. A. 1392 , 82-90, (2015)

Low thermal mass gas chromatography (LTM-GC) was evaluated for rapid, high peak capacity separations with three injection methods: liquid, headspace solid phase micro-extraction (HS-SPME), and direct ...

Post-Translational Modification of Bionanoparticles as a Modular Platform for Biosensor Assembly.

ACS Nano 9 , 8554-61, (2015)

Context driven biosensor assembly with modular targeting and detection moieties is gaining significant attentions. Although protein-based nanoparticles have emerged as an excellent platform for biosen...

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