The Journal of Organic Chemistry

Sulfonation of negatively substituted tert-butylbenzene derivatives

EE Gilbert

Index: Gilbert,E.E. Journal of Organic Chemistry, 1970 , vol. 35, p. 850 - 852

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Citation Number: 8

Abstract

HBr. e EH White, J. Amer. Chem. Soc., 77, 6215 (1955). Monohydrate. methylacetamide and hydrogen chloride, reactionvessel walls became coated with small droplets which rapidly crystallized. Since it seemed reasonable that the liquid might have been the desired amide and the observed crystallization might have been due to increasing contamination with dimethylammonium chloride, vacuum distillation of the amide from the sides of the flask ...

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