An Efficient and Practical Procedure for Synthesis of 1, 1??Diacetates from Aldehydes Catalyzed by Zirconium Sulfate Tetrahydrate–Silica Gel

T Jin, G Feng, M Yang, T Li

Index: Jin, Tongshou; Feng, Guoliang; Yang, Mina; Li, Tongshuang Synthetic Communications, 2004 , vol. 34, # 9 p. 1645 - 1651

Full Text: HTML

Citation Number: 25

Abstract

A facile and efficient procedure for synthesis of 1,1??diacetates from aldehydes with acetic anhydride was described using zirconium sulfate tetrahydrate–silica gel as catalyst in excellent yields under mild reaction conditions. ... A facile and efficient procedure for synthesis of 1,1??diacetates from aldehydes with acetic anhydride was described using zirconium sulfate tetrahydrate–silica gel as catalyst in excellent yields under mild reaction conditions.