The Journal of Organic Chemistry

Convenient and general method for aliphatic and aromatic selenonesters and N-mono-and N, N-disubstituted selenoamides synthesis

VI Cohen

Index: Cohen,V.I. Journal of Organic Chemistry, 1977 , vol. 42, # 15 p. 2645 - 2647

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Abstract

lution under nitrogen. Reactants maintained below 5" C for reaction duration; column chromatographic iso1ation. I conveniently improved by use of high dilution conditions, which were investigated over a 50-fold dilution range. The change in reaction course from a slight modification of reactants and conditions is consistent with our earlier observations' that leaving group, solvent polarity, and temperature could have a critical effect on intrachain ...