The dehydration of secondary and tertiary alcohols

AL Henne, AH Matuszak

Index: Henne; Matuszak Journal of the American Chemical Society, 1944 , vol. 66, p. 1651

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Citation Number: 32

Abstract

Ten secondary and two tertiary alcohols of water at-78'. Fractional distillation was performed in length and complexity have been ddy-adiabatic distilling columns packed with l/, 6” single turn metal helices and equipped with a head of the total reflux-by Of acid reagents, in Order quanti-partial take-off type. As needed, columns were used tatively to determine the identity and ratio of which had a controlled efficiencv of 69. 55. 50 or 45 theo-the resdting olefins. ...

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