All eight stereoisomeric d-glyconic-δ-lactams: synthesis, conformational analysis, and evaluation as glycosidase inhibitors
Y Nishimura, H Adachi, T Satoh, E Shitara…
Index: Journal of Organic Chemistry, , vol. 65, # 16 p. 4871 - 4882
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Citation Number: 50
Abstract
... The Journal of Organic Chemistry. ... d) Ph 3 CCl, (i-Pr) 2 NEt, DMF, rt; (e) Dess−Martin periodinane, CH 2 Cl 2 ; (f) NaBH 4 , MeOH/CH 2 Cl 2 ; (g) (i) (CF 3 SO 2 ) 2 O, Py, CH 2 Cl 2 , −40 °C, (ii) NaN 3 , DMF, rt; (h) H 2 , Raney Ni, MeOH; (i) PPh 3 , CH 3 CN, rt; H 2 O, rt; (j) 4 M ...
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