New syntheses for dilithiotrimethylenemethane: an ionic energy minimum

MM Ludvig, RJ Lagow

Index: Ludvig, Maria M.; Lagow, Richard J. Journal of Organic Chemistry, 1990 , vol. 55, # 16 p. 4880 - 4883

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Citation Number: 5

Abstract

General Conditions. All solvents were dried and distilled under argon before use. Standard Schlenk and vacuum line techniques were used.'H and 13C NMR spectra were taken on either a Nicolet NT-200 or NT-360 instrument. GC/MS were run on a Finnigan 4000 using a 30 m X 0.25 mm Heliflex bonded phase RSL-200 1.0 I. cm capillary column, with an injector temperature of 250" C and an ionizer temperature of 150" C. All thermolysis reactions ...