Syntheses of 5??Chlorouracils/Thymines with 1??[Phosphono (Methyl/Difluoromethyl)]??1, 2??Unsaturated??Moiety??Substituted Methyl Groups at N (1) and Human …
MR Birck, K Clinch, GJ Gainsford…
Index: Helvetica Chimica Acta, , vol. 92, # 5 p. 823 - 838
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Abstract
... of KOH (1.52 g, 27.1 mmol) in 80% aq. MeOH (5 ml) [26]. The solvent was evaporated to low volume, H2O (100 ml) was added and the mixture was washed with CH2Cl2 (2 x 50 ml). The aq. ... ClCO2Et (1.15 ml, Helvetica Chimica Acta – Vol. 92 (2009) 831 Page 10. ...
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