Solid phase synthesis of aminochalcones
F Yi, Y Peng, G Song, J Li
Index: Yi, Fengping; Peng, Yanqing; Song, Gonghua; Li, Jizong Journal of Chemical Research, 2005 , # 5 p. 311 - 312
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Citation Number: 4
Abstract
15min) afforded the corresponding resin-bound amino-chalcones 5ah. In comparison, these reactions need more than 8 h to give similar results under conventional oil bath heating. Because the imine linker is labile under acidic conditions aminochalcones 6ah were finally cleaved from the resin 5ah using 10% TFA/CH2Cl2 for 1.5 h at room temperature. The experimental results are shown in Table 1. ... In conclusion, we have developed a straightforward and efficient ...
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