Tetrahedron

Sequential alkynylation of ω-bromoalkyl triflates: facile access to unsymmetrical non-conjugated diynes including precursors to diene pheromones

RJ Armstrong-Chong, K Matthews, JM Chong

Index: Tetrahedron, , vol. 60, # 45 p. 10239 - 10244

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Citation Number: 12

Abstract

... Tetrahedron. ... The reaction was stirred at 0 °C for 1 h then diluted with hexanes (2×volume of CH 2 Cl 2 ) and filtered through a Celite pad. ... In The Total Synthesis of Natural Products; ApSimon, J., Ed.; Wiley: New York, 1992; Vol. 9, pp 1–534. 2; PN Rylander; ...

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