A tandem denitration-deoxygenation of. alpha.-nitro ketones via (p-tolylsulfonyl) hydrazones with lithium aluminum hydride: a practical synthesis of (Z)-9-tricosene, the …

R Ballini, M Petrini, G Rosini

Index: Ballini, Roberto; Petrini, Marino; Rosini, Goffredo Journal of Organic Chemistry, 1990 , vol. 55, # 17 p. 5159 - 5161

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Citation Number: 14

Abstract

'H NMR spectra were recorded with Bruker WH-360 and AC2OOE spectrometers at 360 and 200 MHz, respectively, with CDC13 as solvent and Me4Si as an internal standard. The 19F NMR spectra were measured at 338.8 MHz and are reported in parts per million upfield from CFC13, which served as both solvent and internal standard. The proton broad-band- decoupled 13C NMR spectra were recorded on the Bruker ACPOOE spectrometer at ...