Development and application of a continuous microwave reactor for organic synthesis

T Cablewski, AF Faux, CR Strauss

Index: Cablewski, Teresa; Faux, Alan F.; Strauss, Christopher R. Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3408 - 3412

Full Text: HTML

Citation Number: 232

Abstract

A laboratory-scale continuous microwave reactor (CMR) has been developed and used to conduct organic syntheses routinely, rapidly, and safely in a range of solvents, under pressures up to 1400 kPa and at temperatures up to 200 OC. Advantages and applications of the CMR are discussed, along with the rationale for the design. Reactions carried out with the CMR included nucleophilic substitution, addition, esterification, transesterification, ...

Related Articles:

3-Hydroxy-4-pyrones as Precursors of 4-Methoxy-3-oxidopyridinium Ylides. An Expeditious Entry to Highly Substituted 8-Azabicyclo [3.2. 1] octanes

[Rumbo, Antonio; Mourino, Antonio; Castedo, Luis; Mascarenas, Jose L. Journal of Organic Chemistry, 1996 , vol. 61, # 18 p. 6114 - 6120]

3-Hydroxy-4-pyrones as Precursors of 4-Methoxy-3-oxidopyridinium Ylides. An Expeditious Entry to Highly Substituted 8-Azabicyclo [3.2. 1] octanes

[Journal of Organic Chemistry, , vol. 61, # 18 p. 6114 - 6120]

3-Hydroxy-4-pyrones as Precursors of 4-Methoxy-3-oxidopyridinium Ylides. An Expeditious Entry to Highly Substituted 8-Azabicyclo [3.2. 1] octanes

[Journal of Organic Chemistry, , vol. 61, # 18 p. 6114 - 6120]

Interaction between the low molecular mass components of blood serum and the VO (iv)–DHP system (DHP= 1, 2-dimethyl-3-hydroxy-4 (1 H)-pyridinone)

[Buglyo, Peter; Kiss, Tamas; Kiss, Erzsebet; Sanna, Daniele; Garribba, Eugenio; Micera, Giovanni Journal of the Chemical Society, Dalton Transactions, 2002 , # 11 p. 2275 - 2282]

Efficient syntheses of N-alkyl-3-hydroxy-2-methyl-4 (1H)-pyridinones from carbohydrate precursors

[Synthetic Communications, , vol. 29, # 6 p. 989 - 1001]

More Articles...