Synthesis of a radiolabelled retinoid X receptor (RXR) specific ligand

P Held, MP Heck, J Iyer, H Gronemeyer…

Index: Held, Pierre; Heck, Marie-Pierre; Iyer, Jaya; Gronemeyer, Hinrich; Lebeau, Luc; Mioskowski, Charles Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 39, # 6 p. 501 - 507

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Abstract

Abstract Synthesis of 4-[2-(5, 5, 8, 8-tetramethyl-5, 6, 7, 8-tetrahydro-naphthalen-2-yl)-[1, 3] dioxolan-2-yl]-benzoic acid or SR11237, a specific ligand of Retinoid X Receptors, is described in a 3 H-labelled version. The labelled retinoid was prepared in 5 steps and tritium was introduced through a final reduction of an aromatic dihalide moiety with 3 H 2.© 1997 John Wiley & Sons, Ltd.

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