Liebigs Annalen der Chemie

Pheromone Synthesis, CLIV. Synthesis of the Stereoisomers of 3??Methyl??4??octanol to Determine the Absolute Configuration of the Naturally Occurring (3S, 4S)?? …

K Mori, H Kiyota, D Rochat

Index: Liebigs Annalen der Chemie, , # 8 p. 865 - 870

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Abstract

... Liebigs Ann. Chem. ... (2 R,3S,2'RS) -1 - (tert- Butyldiphenylsilyloxy) -3-methyl-2- (tetra- hydro-2'H-pyran-2'-yloxy)heptane (18): To a solution of 11 (2.20 g, 6.14 mmol) and 4-(dimethy1amino)pyridine (20 mg) in dry pyridine (8 ml) was added p-toluenesulfonyl chloride ( ...