THE FORMATION OF BENZALDEHYDE AND 2, 4, 6-TRIBROMOANILINE FROM 3, 5-DIBROMO-4-AMINOBENZHYDROL BY THE ACTION OF BROMINE.

L Clarke, GJ Esselen Jr

Index: Clarke; Esselen Journal of the American Chemical Society, 1911 , vol. 33, p. 1138

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Citation Number: 3

Abstract

Five grams of 4-aminobenzhydrol (prepared by reducing 4-aminobenzophenone with sodium amalgam in alcoholic solution) were dissolved in 150 cc. of washed and dried chloroform and to the solution 4 grams (two atoms) of bromine were added. A precipitate was thrown do: w and soon clotted together to form what appeared under a magnifying glass as a mixture of yellowish crystals and a yellow tarry mass. This precipitate was filtered off ...