Preparation and reaction of 1-(methylthio-and phenylthio) vinyllithium reagents.

…, H Furukawa, M Fujimori, K Suzuki, T Fujiwara

Index: Takeda, Takeshi; Furukawa, Hiroyuki; Fujimori, Mizue; Suzuki, Kouichi; Fujiwara, Tooru Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 7 p. 1863 - 1869

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Citation Number: 35

Abstract

1866 were uncorrected. NMR spectra were recorded with JEOL JNM-C-GOHL spectrometer. IR spectra were measured with a JASCO DS-403G spectrometer. 2—Methoxyalkyl Sulfide (I). Phenyl (or methyl) 2- methoxyalkyl sulfides (lb, c, d, e, f, and g) were synthesized by the methylation (Mel/NaH/THF) of the correspond- ing 2-hydroxyalkyl sulfides prepared from aldehydes by the methods reported by Corey and Seebach,” and Peterson!” The boiling points, spectral ...