New Compounds. p, p-Dichlorobenzohydryl 3, 5-Dinitrobenzoate

O Grummitt, A Buck, R Joseph

Index: Grummitt; Buck; Joseph Journal of the American Chemical Society, 1945 , vol. 67, p. 693

Full Text: HTML

Citation Number: 2

Abstract

Three grams (12 millimoles) of p,, p'-dichlorobenzohydrol (prepared by the reduction of p, p- dichlorobenzophenone with zinc and sodium hydroxide') was dissolved in 15 cc. of dry chloroform and 5 cc. of concentrated sulfuric acid was added slowly dropwise with vigorous stirring. After standing at. room temperature for ten minutes the brown mixture was poured onto 50-60 g. of ice. The chloroform layer was separated, washed with 5% sodium ...