Synthetic Communications

Preparation of Benzyl γ-Benxoyloxybutyrates

J Quick, JK Crelling

Index: Quick,J.; Crelling,J.K. Synthetic Communications, 1978 , vol. 8, p. 181 - 186

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Abstract

Abstract As part of our investigation of intramolecular phenolic coupling reactions we required a series of diesters of the general structure, 5 1. Since esters of γ-hydroxybutyric acid have been prepared by acid2 or base3 catalyzed alcoholysis of γ-butyrolactone, it appeared that the desired esters might be prepared by alcoholysis of the lactone with a benzyloxide followed by trapping the new alkoxide, 1, with an acyl chloride. However, ...