A Synthesis of Substituted α-Naphthoquinones
CF Koelsch, DJ Byers
Index: Koelsch; Byers Journal of the American Chemical Society, 1940 , vol. 62, p. 560
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Citation Number: 17
Abstract
Hexamethylmannito1.-Ten grams of tetramethylmannito1 was methylated according to the method of West and Holden. The product obtained was a colorless sirup which distilled at a bath temperature of 95'under 2 mm. pressure;[a]" D+ 12.53'(no solvent), nalD 1.4403, density 1.0458. For comparison 10 g. of isolated mannitol was methylated in the above fashion. The resulting product was found to distil at 97'under 2 mm. pressure;[a]" D+ 12.46' ...
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