Preparation of soluble and insoluble polymer supported IBX reagents

…, M Delgado, K Hereford, B Clapham, KD Janda

Index: Reed, Neal N; Delgado, Mercedes; Hereford, Kristina; Clapham, Bruce; Janda, Kim D Bioorganic and medicinal chemistry letters, 2002 , vol. 12, # 15 p. 2047 - 2049

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Citation Number: 75

Abstract

A series of soluble and insoluble polymer supported versions of the versatile oxidizing reagent IBX has been prepared. Each of the reagents were evaluated for their efficiency in the conversion of benzyl alcohol to benzaldehyde. Results from this study were that the soluble, non-crosslinked polystyrene supported IBX reagent gave the best rate of conversion to benzaldehyde, while the macroporous polymer supported IBX resin provided a superior ...