Resolution of enantiomers of [α-hydroxy-(o-chlorophenyl) methyl] phosphinic acid via diastereomeric salt formation with enantiopure 1-phenylethylamines
B Kaboudin, S Alaie, T Yokomatsu
Index: Kaboudin, Babak; Alaie, Saied; Yokomatsu, Tsutomu Tetrahedron Asymmetry, 2011 , vol. 22, # 18-19 p. 1813 - 1816
Full Text: HTML
Citation Number: 10
Abstract
The resolution of racemic α-hydroxy-H-phosphinic acid with enantiopure 1- phenylethylamines via diastereomeric salt formation was investigated. X-Ray crystallographic analysis of the salt revealed that (R)-1-phenylethylamine to be efficient resolving agent for obtaining a single enantiomer of [α-hydroxy-(o-chlorophenyl) methyl] phosphinic acid. Resolving racemic α-hydroxy-H-phosphinic acid with (S)-2- ...
Related Articles:
[Vassiliou, Stamatia; Grabowiecka, Agnieszka; Kosikowska, Paulina; Berlicki, Lukasz Arkivoc, 2012 , vol. 2012, # 4 p. 33 - 43]
1??hydroxy??1, 1??bis (H??phosphinates): Synthesis, stability, and sorption properties
[David, Tomas; Kreckova, Pavlina; Kotek, Jan; Kubicek, Vojtech; Lukes, Ivan Heteroatom Chemistry, 2012 , vol. 23, # 2 p. 195 - 201]