Alkylfluorophenylcarbinols with Choleretic Activity
NP Buu-Hoi, ND Xuong, BK Diep…
Index: Buu-Hoi,N.P. et al. Journal of Organic Chemistry, 1962 , vol. 27, p. 2669 - 2670
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Abstract
1 1 I 1 I 4000 3000 2000 1500 1000 goo eon 700 ... I I I 4000 3WO 2000 1SW 1000 900 800 7w WVENUMBERS i rm-' Figure 2 ... Experimental 6-Chloropenicillanic Acid (Ia).-A solution of 6.5 g. of 6-APA in 100 ml. of 1 N hydrochloric acid waa cooled to 0-2" and a solution of 2.5 g. of sodium nitrite in 20 ml. of water waa added dropwise. One hour after the completion of the addition, the temperature was allowed to rise to 15-18' and the separated oil extracted ...
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