Pressure effects in a solvolysis involving extended. pi. participation
NH Ho, WJ Le Noble
Index: Ho, Nan-hui; Noble, W. J. le Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 2018 - 2021
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Citation Number: 20
Abstract
Table IV. Reaction of Hexanal with MerSiNCSe" solvent catalyst time, h temp, "C yield,b 70 CH3CN - 48 RT' <1 ZnClzd 24 40 - 15 ... Reactions were carried out with Me3SiNCSe (5 mmol), hexanal (5 mmol), and a solvent (10 mL). bDetermined by GLC with n- tridecane as an internal standard. Room temperature. 0.3 mmol. ... Table V. One-Pot Reaction of Hexanal with Me,SiNCSe in Various Solventsn solvent catalyst time, h temp, "C yield,b 70 CH3CN ZnClZC 48 RTe ...
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