Tetrahedron letters

A real time reaction monitoring using fluorescent dansyl group as a solid-phase leaving group

T Suenaga, C Schutz, T Nakata

Index: Suenaga, Toshiro; Schutz, Caroline; Nakata, Tadashi Tetrahedron Letters, 2003 , vol. 44, # 31 p. 5799 - 5801

Full Text: HTML

Citation Number: 6

Abstract

A real time monitoring method to monitor the progress of the solid-phase reaction has been developed. The substitution reaction on the solid-phase was clearly monitored as a change in the color depth using the fluorescent dansyl group as the leaving group. This methodology is applicable to both parallel and split combinatorial synthesis.

Related Articles:

A novel and highly selective conversion of alcohols, thiols, and silyl ethers to azides using the triphenylphosphine/2, 3-dichloro-5, 6-dicyanobenzoquinone (DDQ)/n- …

[Iranpoor, Nasser; Firouzabadi, Habib; Akhlaghinia, Batool; Nowrouzi, Najmeh Tetrahedron Letters, 2004 , vol. 45, # 16 p. 3291 - 3294]

Stereoretentive halogenations and azidations with titanium (IV) enabled by chelating leaving groups

[Lepore, Salvatore D.; Mondal, Deboprosad; Song, Ye Li; Bhunia, Anjan K. Angewandte Chemie - International Edition, 2008 , vol. 47, # 39 p. 7511 - 7514]

Histone deacetylase inhibitors through click chemistry

[Shen, Jie; Woodward, Robert; Kedenburg, James Patrick; Liu, Xianwei; Chen, Min; Fang, Lanyan; Sun, Duxin; Wang, Peng George Journal of Medicinal Chemistry, 2008 , vol. 51, # 23 p. 7417 - 7427]

Copper??in??Charcoal??Catalyzed, Tandem One??Pot Diazo Transfer??Click Reactions

[Lee, Ching-Tien; Huang, Shenlin; Lipshutz, H. Bruce Advanced Synthesis and Catalysis, 2009 , vol. 351, # 18 p. 3139 - 3142]

Reductive Azidation of Carbonyl Compounds via Tosylhydrazone Intermediates Using Sodium Azide

[Barluenga, Jose; Tomas-Gamasa, Maria; Valdes, Carlos Angewandte Chemie - International Edition, 2012 , vol. 51, # 24 p. 5950 - 5952]

More Articles...