Molecules

A Comparison of Microwave-Accelerated and Conventionally Heated Iodination Reactions of Some Arenes and Heteroarenes, Using ortho-Periodic Acid as …

M Sosnowski, L Skulski

Index: Sosnowski, Maciej; Skulski, Lech Molecules, 2005 , vol. 10, # 2 p. 401 - 406

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Citation Number: 13

Abstract

Abstract: A fast and simple method for the oxidative iodination of some activated arenes and heteroarenes, either under microwave irradiation or by conventional heating, is reported, using diiodine and ortho-periodic acid as the oxidant. The reactions were carried out in hot 95% ethanol under a reflux condenser. For the microwave assisted reactions, the reaction times were always notably shortened, but the yields were nearly the same as those ...