Journal of Chemical and Engineering Data

Reaction of 4, 6-diarylhexahydro-1, 3, 5-triazine-2-thiones with. alpha.-haloketones. 3

AAW Soliman

Index: Soliman, Adly Abdel-Wahid Journal of Chemical & Engineering Data, 1984 , vol. 29, # 1 p. 99 - 101

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Citation Number: 3

Abstract

2-[(Phenylthlocarbamoyl) am/no 1-2, 3-d/hydrobenz-~/d~~ e-7, 3-d/carbothloamMe(6). A 8.35-g sample of 1 and 15 g of potassium phthailmide were mixed in a porcelain mortar. The reagents were heated at 200 OC for 2 h. The product was cooled and dissolved in 100 cm3 of methanol, and 10 cm3 of 80% aqueous hydrazine was added. The reagents were stirred under reflux for 3 h. The precipitate was filtered and the filtrate was neutralized with KOH. ...