Tetrahedron letters

Simple method for the introduction of iodo-label on (3-trifluoromethyl) phenyldiazirine for photoaffinity labeling

M Hashimoto, Y Kato, Y Hatanaka

Index: Hashimoto, Makoto; Kato, Yuhi; Hatanaka, Yasumaru Tetrahedron Letters, 2006 , vol. 47, # 20 p. 3391 - 3394

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Citation Number: 12

Abstract

A simple and mild method was developed for the introduction of iodo-label on (3- trifluoromethyl) phenyldiazirine (TPD) aromatic ring in the presence of three membered diazirine ring. An iodination protocol, I2–BTI in CH3CN, was found to be effective even though affinity ligands are pre-installed.

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