Facile method for trimethylsilylation of alcohols using hexamethyldisilazane and ammonium thiocyanate under neutral conditions

…, KSA Kumar, VD Chaudhari, DD Dhavale

Index: Jadhav, Vrushali H.; Kumar, K. S. Ajish; Chaudhari, Vinod D.; Dhavale, Dilip D. Synthetic Communications, 2007 , vol. 37, # 8 p. 1363 - 1370

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Citation Number: 11

Abstract

A highly efficient method for trimethylsilylation of primary, secondary, tertiary, allylic, and a variety of sugar??derived alcohols using hexamethyldisilazane in the presence of a catalytic amount of ammonium thiocyanate under neutral conditions is reported. ... A highly efficient method for trimethylsilylation of primary, secondary, tertiary, allylic, and a variety of sugar??derived alcohols using hexamethyldisilazane in the presence of a catalytic amount of ammonium ...