Action of 9-Diazofluorene on ι-Nitrostyrenes and its Substituted Derivatives

A Mustafa, AHE Harhash

Index: Mustafa; Harhash Journal of the American Chemical Society, 1954 , vol. 76, p. 1383

Full Text: HTML

Citation Number: 5

Abstract

1, 2-Diphenyl-l-chlorornercuripropanol-2.-To a suspension of 3.0 g.(0.0155 mole) of trans-a- methylstilbenes (mp 80.5-81.5', diffraction [20] 4.88;[16] 6.96, 6.48;[12] 4.52, 3.86;[lo] 4.68;[8] 3.79; 161 3.71;[4] 11.78, 3.25;[2] 5.86;[l] 7.52, 4.35, 4.02) and 9.6 g.(0.031 mole) of mercuric acetate in 125 ml. of 50% aqueous 1, 2-dimethoxyethane was added 1.00 g.(0.004 mole) of benzoyl peroxide. After 6 days agitation at 20-25'the system was filtered into 200 ml. of 3% ...