A three-carbon condensative expansion. Application to muscone
BM Trost, JE Vincent
Index: Trost, Barry M.; Vincent, John E. Journal of the American Chemical Society, 1980 , vol. 102, # 17 p. 5680 - 5683
Full Text: HTML
Citation Number: 95
Abstract
13k 14 15 16 a See ref 5 and 6.(a) 3, NaH, 1 equiv of NaI, DMF, 55" C, 2-12 h.(b) 3, NaH, 0.2 equiv of NaI, DME, 65" C, 36 11.(c) 0.2 cquiv of (C, H,), NF, THF, 55" C, 1 h.(d) KH, 1 equiv of 18-crown-6, DME, room temp, 2-5 h.(e) 0.2 equiv of (C, H,), NF, THF, 55" C, 30 min.(f) PhCH,, reflux, 48 h. e) 0.4 equiv of (C, H,), NF, THF, 55" C, 3 h then DBU, CH, Cl,, reflux, 1 h.(h) mp 115-116" C.(i) mp 139-139.5" C.(i) mp 114-1 15" C, 17= 2.(k) mp 55-60" C and ...
Related Articles:
Diastereoselective sulfenylation reactions employing N-phenylthio lactams under nonbasic conditions
[Wilson, Lawrence J.; Liotta, Dennis C. Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 1948 - 1950]
[Vankar, Yashwant D.; Shah, Kavita; Bawa, Anita; Singh, Surendra P. Tetrahedron, 1991 , vol. 47, # 42 p. 8883 - 8906]
New mild methodology for the synthesis of α-phenylthio and α-phenylseleno ketones
[Magnus, Philip; Rigollier, Pascal Tetrahedron Letters, 1992 , vol. 33, # 41 p. 6111 - 6114]
Iodomethyl phenyl sulfoxide: reactivity and synthetic applications
[Reutrakul, Vichai; Panyachotipun, Chitchanun; Hahnvajanawong, Viwat; Sotheeswaran, S. Tetrahedron Letters, 1984 , vol. 25, # 17 p. 1825 - 1828]
Iodomethyl phenyl sulfoxide: reactivity and synthetic applications
[Reutrakul, Vichai; Panyachotipun, Chitchanun; Hahnvajanawong, Viwat; Sotheeswaran, S. Tetrahedron Letters, 1984 , vol. 25, # 17 p. 1825 - 1828]