Journal of fluorine chemistry

A new route to polyfluorinated trifluoromethanesulfonates. Synthesis of perfluoroallyl and perfluorobenzyl triflates

VA Petrov

Index: Journal of Fluorine Chemistry, , vol. 73, # 1 p. 17 - 20

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Citation Number: 6

Abstract

... triflate (10-20 mmol) was added dropwise to a stirred, equimolar solution of KI or KOCF(CF3)2 [prepared from (CF3)2C=O and KF] in diglyme at 0 °C at a rate sufficient to keep the temperature below 25 °C. After 1 h at ... I(.A. Petrov / Journal of Fluorine Chemistry 73 (1995) ...