The Journal of Organic Chemistry

New highly fluorescent derivative of adenosine. Cyclization of adenosine with 1'-methylthiaminium ion

JA Zoltewicz, TD Baugh

Index: Zoltewicz, John A.; Baugh, Thomas D. Journal of Organic Chemistry, 1982 , vol. 47, # 7 p. 1352 - 1354

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Abstract

(8) As the larger columns are run under vacuum, additional solvent can be run in as needed. Thus, the column need only be tall enough to contain the initial silica gel slurry. The 120-mm- diameter column is 210 mm long, and the 170-mm-diameter column is 270 mm long.(9) Use of vacuum-driven column chromatography has previously been described: Targett, NM; Kilcoyne, JP; Green, BJ Org. Chem. 1979,