Stereo-and photochemistry of 1, 2, 3, 4, 5-pentaphenyl-1, 3, 5-heptatriene

…, LJ Radonovich, FM Saad, M Brostrom

Index: Woolsey, Neil F.; Radonovich, Lewis J.; Saad, Fathi M.; Brostrom, Myles Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 1937 - 1941

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Citation Number: 2

Abstract

Experimental Section All materials used were obtained from commercial sources and were not purified deuterated methanol (Sigma), quadricyclane (Aldrich), stannous chloride (Fischer), palladium chloride (Alfa), p-dichlorbenzene (Fischer). 'H NMR spectra were recorded at 60 MHz on a JEOL-FXGOQ pulsed NMR spectrometer. A spectral with width of 600 Hz was used with a single 90' pulse and 8K bits of data collection. Probe temperatures were measured with a ...