Dalton Transactions

Palladium (ii) thiocarboxamide complexes: synthesis, characterisation and application to catalytic Suzuki coupling reactions

E Sindhuja, R Ramesh, Y Liu

Index: Sindhuja, Elangovan; Ramesh, Rengan; Liu, Yu Dalton Transactions, 2012 , vol. 41, # 17 p. 5351 - 5361

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Citation Number: 24

Abstract

A simple route to synthesise palladium (II) complexes from the reaction of N-substituted pyridine-2-thiocarboxamide ligands and PdCl2 (PPh3) 2 has been developed. The new complexes are very soluble in common solvents and have been fully characterised (elemental analysis, FT-IR, 1H, 31P, 13C-NMR), including an X-ray diffraction analysis. The molecular structures of all the complexes were determined and reveal the presence of ...

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