Growth and characterization of thiosemicarbazide hydrochloride: A semiorganic NLO material

R Santhakumari, K Ramamurthi, RR Babu…

Index: Santhakumari; Ramamurthi; Babu, R. Ramesh; Evans, Helen Stoeckli; Bhagavannarayana; Hema Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2011 , vol. 82, # 1 p. 102 - 107

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Citation Number: 6

Abstract

Thiosemicarbazide hydrochloride (TSCHCL) was synthesized by mixing thiosemicarbazide and hydrochloride in 1: 1 molar ratio in double distilled water. Single crystals of TSCHCL were grown by slow evaporation at room temperature and were characterized by single crystal X-ray diffraction study to determine the molecular structure and by FT-IR, 1H and 13C NMR spectral analyses to confirm the synthesized compound. Thermogravimetric and ...