Anodic behavior of crowded triarylphosphines. ESR study of triarylphosphoniumyl radicals, Ar3P. bul.+

M Culcasi, Y Berchadsky, G Gronchi…

Index: Journal of Organic Chemistry, , vol. 56, # 11 p. 3537 - 3542

Full Text: HTML

Citation Number: 68

Abstract

... The reaction mixture was stirred for 1 h at -25 OC and kept overnight at room temperature; saturated aqueous NH4C1 was then added, and the organic layer was washed with 1 N HC1 (15 mL) and saturated brine (15 mL). ... Page 2. 3638 J. Org. Chem., Vol. 56, No. 11, 1991 ...