The one-pot halomethylation of 5-substituted salicylaldehydes as convenient precursors for the preparation of heteroditopic ligands for the binding of metal salts
Q Wang, C Wilson, AJ Blake, SR Collinson, PA Tasker…
Index: Wang, Qiang; Wilson, Claire; Blake, Alexander J.; Collinson, Simon R.; Tasker, Peter A.; Schroeder, Martin Tetrahedron Letters, 2006 , vol. 47, # 50 p. 8983 - 8987
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Citation Number: 35
Abstract
The one-pot bromo-and chloro-methylation of various 5-substituted salicylaldehydes with paraformaldehyde and hydrobromic or hydrochloric acid has been achieved. This approach establishes a convenient and flexible method to attach functional arms to salicylaldehydes for further applications in organic and coordination chemistry. Examples are described using 3-bromomethyl-5-t-butylsalicylaldehyde in the synthesis of piperazine-containing ...
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