Neurotrope und psychotrope substanzen XI. Über die synthese von 3, 8-difluor-11-(3-dimethylaminopropyliden)-6, 11-dihydrodibenzo [b, e] thiepin

M Rajšner, M Protiva

Index: Collection of Czechoslovak Chemical Communications, , vol. 32, # 5 p. 2021 - 2024

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Abstract

... Der Riickstand wurde mit 60 ml Benzol vermischt und das feste Produkt abgesaugt; 32 g; Smp. ... Collection Czechosiov. ... der Extrakt getrocknet und verdampft; es fiel ein zweiter Anteil an (3,5 g). Beide Anteile wurden vereint (9,4 g) und aus ·22 ml Benzol umkristallisiert; 5,5 g, Smp ...

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