Organic Letters

TiCl4/Et3N-Mediated Condensation of Acetate and Formate Esters: Direct Access to β-Alkoxy-and β-Aryloxyacrylates

JM Álvarez-Calero, ZD Jorge, GM Massanet

Index: Ziegler, Thomas; Moehler, Hans; Effenberger, Franz Chemische Berichte, 1987 ,  vol. 120, p. 373 - 378

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Abstract

... The above problem was solved with a slight increase of both TiCl 4 and Et 3 N (entry 9, Table 1). Finally, the use of one-half of the volume of solvents in the workup produced the same result (entry 10, Table 1). ... e Workup using half of the volume of the solvents. ...